Synthesis of thioamides on the basis of biogenic amines, aromatic aldehydes and sulfur

  • Zh. Аkhmetkarimova Institute of organic synthesis and coal chemistry
  • D. Zhienbaeva Institute of organic synthesis and coal chemistry
  • S. Fazylov Institute of organic synthesis and coal chemistry
  • О. Nurkenov Institute of organic synthesis and coal chemistry

Abstract

N–substituted thiamides of benzoic acid were obtained by interaction between arilaldehydes and secondary amines (morpholine, 1–benzylpiperazine and sulfur in the conditions of Willgerodt–Kindler reaction and in terms of microwave activation.

References

1. Машковский М.Д., Лекарственные средства, – М.:ООО РИА «Новая волна», 15–е издание, 2007. – C.1206.
2. Padma A., Beal L.S., Heidelbaugh T.M. and ets. // J. Org. Chem. – 2000. – Vol.65. –P.2684– 2686.
3. Wipf P., Venkatraman S.J. // J. Org. Chem. –1996. – Vol.61. –P.8004–8006.
4. Thiazole and its Derivatives. Part 1. // J. Wiley and Sons Inc. –1979. –P.115–130.
5. Мельников Н.Н., Волков А.И., Короткова О.А. Пестициды и окружающая среда. – М.: Химия, 1977. – C.240.
6. Эльдерфилд Р. Гетероциклические соединения. – Издательство ИЛ: Москва, – 1960. – Т.5. – С.401.
7. Петров К.А., Андреев Л.Н. // Усп. химии. –1969. –Т.38. – С.41–52.
8. McManus S.P., Lee K.Y., Pittman C.U. // J. Org. Chem. – 1974. – Vol.39. –P.3041–3043.
9. Jagodzinski T.S. // Chem. Rev. – 2003. – Vol.103. – P.197–199.
10. Kappe C.O., Stadler A. Microwaves in Organic and Medicinal Chemistry. – Weinheim:Wiley–VCH, 2005. – P.410. https://doi.org/10.1002/3527606556
11. Рахманкулов Д. Л., Шавшукова С. Ю. Создание микроволновой техники в 1940– 1970–х годах. // История науки и техники. –2008. –№3. –Вып.1. – С.52–55.
12. Villemin D., Martin В., Bar N. Application of Microwave in Organic Synthesis. Dry Synthesis of 2–Arylmethylene–3(2)–naphthofuranones // Molecules. –1998. –Vol.3. –P.88–93.
Published
2011-03-30
How to Cite
АkhmetkarimovaZ., Zhienbaeva, D., Fazylov, S., & NurkenovО. (2011). Synthesis of thioamides on the basis of biogenic amines, aromatic aldehydes and sulfur. Chemical Bulletin of Kazakh National University, 61(1), 337-340. Retrieved from https://chemistry.kz/bulletin/index.php/kaznu/article/view/933