Study of the iron nanoparticles phase transformation during thermal annealing

  • Artem Leonidovich Kozlovskiy L.N. Gumilyov Eurasian National University, Astana
  • Jumat Beisembekovich Kargin L.N. Gumilyov Eurasian National University, Astana
  • Malik Zhenisovich Kokarev L.N. Gumilyov Eurasian National University, Astana
  • Daut Galimzhanovich Mukhambetov Almaty Academy of Economic and Statistics, Almaty
DOI: https://doi.org/10.15328/cb796
Keywords: nanostructures; mechanochemical synthesis; thermal annealing; phase transformations; nanoparticles

Abstract

Change in structural properties and phase composition of nanoparticles based on iron oxide was researched in the paper. As a result of conducted studies it was found that during heat treatment oxide phases of (γ-Fe2O3) and α-Fe2O3 maghemite were formed in oxygen atmosphere. Researches of powder array magnetization were showed that the hysteresis loop movement had the form characteristic for ferromagnetic materials. Additionally, loops obtained at different directions of the magnetic field have different characters, which indicate the magnetic anisotropy presence in the samples.

Author Biography

Artem Leonidovich Kozlovskiy, L.N. Gumilyov Eurasian National University, Astana

Institute of Nuclear Physics, Almaty

References

1 Yen SK, Padmanabhan P, Selvan ST (2013) Theranostics 3:986-1003. Crossref

2 Hulteen JC, Martin CR (1997) J Mater Chem 7:1075-1087. Crossref

3 Kalska-Szostko B, Orzechowska E, Wykowska U (2013) Colloids Surfaces B Biointerfaces 111:509-516. Crossref

4 Ahmad Umar, Abaker M (2011) J Nanosci Nanotechno 11:3474-3480. Crossref

5 Ani Idris, Nur Suriani Mohd (2012) J Ind Eng Chem 18:1582-1589.

6 Liu SQ (2012) Environ Chem Lett 10:209-216. Crossref

7 Lakouraj MM, Norouzian RS, Balo S (2015) J Chem Eng Data. 60:2262-2272. Crossref

8 Harsha N, Krishna KVS, Renuka NK, Shukla S. (2015) RSC Adv 5:30354-30362. Crossref

9 Houas A, Lachheb H, Ksibi M, Elaloui E, Guillard C, Herrmann JM. (2001) Appl Catal B. 31:145-157. Crossref

10 Abramson S, Srithammavanh L, Siaugue JM, Horner O (2009) J Nanopart Res 1:459-465. Crossref

11 Lorencon E, Brandao FD, Krambrock K, Alves DCB (2014) J Mol Catal A 394:316-323. Crossref

12 Wu Ch, Chen D (2012) Nanoscale Res Lett 7:317. Crossref

13 Pozun ZD, Rodenbusch SE, Keller E (2013) J Phys Chem C 117:7598-7604. Crossref

14 Ikeda О, Ohnuma I, Kainuma R, Ishida K (2001) Intermetallics 9:755-761. Crossref

15 Tolstoi VP (1993) Russ Chem Rev 62:237. Crossref

16 Klimov VI, Kurz H, Karavanskii VA (1995) Appl Phys Lett 67:653. Crossref

17 Kozlovskiy A, Zhanbotin A, Zdorovets M, Rusakov VS (2016) Nucl Instrum Meth B 381:103-109. Crossref
Published
2017-03-31
How to Cite
Kozlovskiy, A., Kargin, J., Kokarev, M., & Mukhambetov, D. (2017). Study of the iron nanoparticles phase transformation during thermal annealing. Chemical Bulletin of Kazakh National University, 84(1), 16-25. https://doi.org/https://doi.org/10.15328/cb796
Issue
Vol 84 No 1 (2017): Chemical Bulletin of Kazakh National University
Section
Physical Chemistry and Electrochemistry
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